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Solvent-induced selectivity of Williamson etherification in the pursuit of amides resistant against oxidative degradation

https://doi.org/10.1039/d0ra04465b

Derr, James B. ; Clark, John A. ; Morales, Maryann ; Espinoza, Eli M. ; Vadhin, Sandra ; Vullev, Valentine I. ( June 2020 , RSC Advances)

This article reports two discoveries. (1) 2-Methoxyethanol induces unprecedented selectivity for etherification of 5-hydroxy-2-nitrobenzic acids without forming undesired esters. (2) Such compounds are precursors for amides showing unusual robustness against oxidative degradation, essential for molecular electrets that transfer strongly oxidizing holes at about −6.4 eV vs. vacuum.
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Engineering orthogonal human O-linked glycoprotein biosynthesis in bacteria

https://doi.org/10.1038/s41589-020-0595-9

Natarajan, Aravind ; Jaroentomeechai, Thapakorn ; Cabrera-Sánchez, Marielisa ; Mohammed, Jody C. ; Cox, Emily C. ; Young, Olivia ; Shajahan, Asif ; Vilkhovoy, Michael ; Vadhin, Sandra ; Varner, Jeffrey D. ; et al ( October 2020 , Nature Chemical Biology)

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